C₂₃H₂₂FNO₆S

Base Information Edit

Chemical Name:C₂₃H₂₂FNO₆S
CAS No.:1374234-59-9
Molecular Formula:C₂₃H₂₂FNO₆S
Molecular Weight:459.495
Hs Code.:
Mol file:1374234-59-9.mol

C<sub>23</sub>H<sub>22</sub>FNO<sub>6</sub>S

Synonyms:C₂₃H₂₂FNO₆S

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Chemical Property of C₂₃H₂₂FNO₆S Edit

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Technology Process of C₂₃H₂₂FNO₆S

There total 7 articles about C₂₃H₂₂FNO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1374234-58-8
C₂₃H₂₀FNO₆S

: 1374234-59-9
C₂₃H₂₂FNO₆S

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 2h;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374234-59-9
C₂₃H₂₂FNO₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

4.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

4.2: 0.5 h / 20 °C

5.1: pyridine / 1 h / 0 - 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

6.2: 2 h / 60 °C

7.1: sodium tetrahydroborate / ethanol / 2 h / 0 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; tin(II) chloride dihdyrate; water; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374234-59-9
C₂₃H₂₂FNO₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

5.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

5.2: 0.5 h / 20 °C

6.1: pyridine / 1 h / 0 - 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

7.2: 2 h / 60 °C

8.1: sodium tetrahydroborate / ethanol / 2 h / 0 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; tin(II) chloride dihdyrate; water; boron trichloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;