3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose

Base Information

• Chemical Name: 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose
• CAS No.: 97576-84-6
• Molecular Formula: C₆₁H₆₄O₁₁
• Molecular Weight: 973.173

Synonyms:3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose

Chemical Property of 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose

There total 23 articles about 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-methoxyethyl O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-benzyl-β-D-glucopyranoside → O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-benzyl-D-glucopyranose (93495-91-1,97576-84-6)

Guidance literature:

With titanium tetrachloride; In dichloromethane;

DOI:10.1246/bcsj.65.3257

Reference yield: 64.0%

2-methoxyethyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-benzyl-β-D-glucopyranoside → O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-benzyl-D-glucopyranose (93495-91-1,97576-84-6)

Guidance literature:

With titanium tetrachloride; In dichloromethane;

DOI:10.1246/bcsj.65.3257

Reference yield: 59.0%

allyl 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside (97576-83-5) → 3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranose (97576-84-6)

Guidance literature:

With palladium dichloride; In methanol; at 20 ℃; for 1h; Irradiation;

DOI:10.1016/0008-6215(85)85192-2

upstream raw materials:

2,3,4,6-tetra-O-benzyl-D-glucopyranose

allyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranoside

2,3,4,6-Tetra-O-benzyl-D-glucopyranose

2-methoxyethyl 3,4,6-tri-O-benzyl-β-D-glucopyranoside

Downstream raw materials:

3,4,6-tri-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranosyl chloride

benzyl O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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