C₁₁H₁₁F₂NO

Base Information

Chemical Name:C₁₁H₁₁F₂NO
CAS No.:798564-59-7
Molecular Formula:C₁₁H₁₁F₂NO
Molecular Weight:211.211
Hs Code.:

C<sub>11</sub>H<sub>11</sub>F<sub>2</sub>NO

Synonyms:C₁₁H₁₁F₂NO

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Chemical Property of C₁₁H₁₁F₂NO

Chemical Property:

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Technology Process of C₁₁H₁₁F₂NO

There total 4 articles about C₁₁H₁₁F₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798564-58-6
C₁₀H₁₁ClF₂O

: 143-33-9,25596-52-5
sodium cyanide

: 798564-59-7
C₁₁H₁₁F₂NO

Guidance literature:: In dimethyl sulfoxide; at 95 ℃; for 1h;

Reference yield:

: 203059-83-0
1,3-difluoro-4-isopropoxybenzene

: 798564-59-7
C₁₁H₁₁F₂NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 0.5 h / -78 - -75 °C

1.2: 0.67 h / -40 - 0 °C

2.1: lithium aluminium tetrahydride; ammonium chloride / tetrahydrofuran / 0.5 h / 0 - 45 °C

3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 23.17 h / 20 - 40 °C / Heating / reflux

4.1: dimethyl sulfoxide / 1 h / 95 °C

With lithium aluminium tetrahydride; sec.-butyllithium; ammonium chloride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; cyclohexane; dimethyl sulfoxide;

Reference yield:

: 798564-57-5
C₁₀H₁₂F₂O₂

: 798564-59-7
C₁₁H₁₁F₂NO

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; triethylamine / dichloromethane / 23.17 h / 20 - 40 °C / Heating / reflux

2: dimethyl sulfoxide / 1 h / 95 °C

With methanesulfonyl chloride; triethylamine; In dichloromethane; dimethyl sulfoxide;