(+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

Base Information

Chemical Name:(+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide
CAS No.:1331783-08-4
Molecular Formula:C₂₉H₂₄F₃O₄PS
Molecular Weight:556.542
Hs Code.:

Synonyms:(+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

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Chemical Property of (+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

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Technology Process of (+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

There total 2 articles about (+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1331782-90-1,1331783-48-2
(+/-)-12-bromo[2.2]paracyclophan-4-yl trifluoromethanesulfonate

: 4559-70-0
Diphenylphosphine oxide

: 1289455-52-2,1331783-12-0,866722-07-8
rac-P-(4-[2.2]paracyclophanyl)-P,P-diphenylphosphine oxide

: 1331783-08-4
(+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

: (+/-)-4,12-bis(diphenylphosphinyl)[2.2]paracyclophane

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 100 ℃; for 4.5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.05.023

Reference yield:

: 1331782-90-1,1331783-48-2
(+/-)-12-bromo[2.2]paracyclophan-4-yl trifluoromethanesulfonate

: 4559-70-0
Diphenylphosphine oxide

: 850262-93-0,850263-06-8
(+/-)-{12-bromo[2.2]paracyclophan-4-yl}diphenylphosphine oxide

: 1331783-08-4
(+/-)-{12-trifluoromethanesulfonyloxy[2.2]paracyclophan-4-yl}diphenylphosphine oxide

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 100 ℃; for 7h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.05.023