11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

Base Information

Chemical Name:11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene
CAS No.:630426-43-6
Molecular Formula:C₅₂H₆₈O₄S₂
Molecular Weight:821.242
Hs Code.:

Synonyms:11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

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Chemical Property of 11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

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Technology Process of 11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

There total 8 articles about 11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 521275-68-3
bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfone

: C₅₂H₆₈O₄S₂

: 630426-43-6
11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

Guidance literature:: With potassium hydroxide; In tetrachloromethane; tert-butyl alcohol; at 20 ℃; for 7h;
DOI:10.1002/hlca.200390211

Reference yield:

: 56691-80-6
geranyl phenyl sulfone

: 630426-43-6
11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / BuLi / tetrahydrofuran; hexane / 0 - 20 °C

2: 75 percent / NaOEt / ethanol / 10 h / Heating

3: 55 percent / LiNbMoO₆; H₂O₂ / methanol; benzene; H₂O / 6 h / 20 °C

4: 90 percent / NaH; NaI / tetrahydrofuran / 15 h / 20 °C

5: 40 percent / urea; H₂O₂; phthalic anhydride / acetonitrile / 5 h / 0 °C

6: KOH / 2-methyl-propan-2-ol; CCl₄ / 7 h / 20 °C

With potassium hydroxide; phthalic anhydride; n-butyllithium; LiNbMoO₆; dihydrogen peroxide; sodium ethanolate; sodium hydride; urea; sodium iodide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; hexane; water; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1002/hlca.200390211

Reference yield:

: 3,7,11-trimethyl-1-(phenylsulfanyl)dodeca-2,4,6,10-tetraene

: 630426-43-6
11,11',12,12'-tetrahydro-11,11'-bis(phenylsulfonyl)lycopene

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / LiNbMoO₆; H₂O₂ / methanol; benzene; H₂O / 6 h / 20 °C

2: 90 percent / NaH; NaI / tetrahydrofuran / 15 h / 20 °C

3: 40 percent / urea; H₂O₂; phthalic anhydride / acetonitrile / 5 h / 0 °C

4: KOH / 2-methyl-propan-2-ol; CCl₄ / 7 h / 20 °C

With potassium hydroxide; phthalic anhydride; LiNbMoO₆; dihydrogen peroxide; sodium hydride; urea; sodium iodide; In tetrahydrofuran; methanol; tetrachloromethane; water; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1002/hlca.200390211