benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

Base Information

Chemical Name:benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside
CAS No.:128848-33-9
Molecular Formula:C₄₁H₅₁IO₁₁
Molecular Weight:846.754
Hs Code.:

benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

Synonyms:benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

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Chemical Property of benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

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Technology Process of benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

There total 5 articles about benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 128848-32-8
benzyl 3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-ioso-α-L-altropyranosyl)-2,6-dideoxy-4-O-(p-methoxybenzyl)-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

: 128848-33-9
benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 0.833333h; Ambient temperature;
DOI:10.1016/S0040-4020(01)97588-X

Reference yield:

: 106988-78-7
1,5-Anhydro-3-O-benzoyl-2,6-didesoxy-4-O-(4-methoxybenzyl)-L-ribo-hex-1-enit

: 128848-33-9
benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1) molecular sieves, 2) N-iodosuccinimide / 1) acetonitrile, 30 min., 2) acetonitrile, RT

2: 66 percent / 1) H₂, NEt₃, 2) NaOCH₃ / 1) 10percent Pd-C / 1) 10 h, RT, 2) MeOH a) 30h, RT, b) 24h, 55 deg C

3: 24 percent / N-iodosuccinimide / acetonitrile / 12 h / Ambient temperature

4: 70 percent / DDQ / CH₂Cl₂; H₂O / 0.83 h / Ambient temperature

With N-iodo-succinimide; molecular sieve; hydrogen; sodium methylate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4020(01)97588-X

Reference yield:

: 128848-18-0
benzyl 3-O-<3-O-benzoyl-2,6-dideoxy-2-iodo-4-O-(p-methoxypbenzyl)-α-L-altropyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

: 128848-33-9
benzyl-3-O-<3-O-(4-O-acetyl-3-O-benzyl-2,6-dideoxy-2-iodo-α-L-altropyranosyl)-2,6-dideoxy-α-L-ribo-hexopyranosyl>-4-O-benzyl-2,6-dideoxy-α-L-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / 1) H₂, NEt₃, 2) NaOCH₃ / 1) 10percent Pd-C / 1) 10 h, RT, 2) MeOH a) 30h, RT, b) 24h, 55 deg C

2: 24 percent / N-iodosuccinimide / acetonitrile / 12 h / Ambient temperature

3: 70 percent / DDQ / CH₂Cl₂; H₂O / 0.83 h / Ambient temperature

With N-iodo-succinimide; hydrogen; sodium methylate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4020(01)97588-X