benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside

Base Information

• Chemical Name: benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside
• CAS No.: 81997-64-0
• Molecular Formula: C₂₂H₂₈N₂O₄
• Molecular Weight: 384.475

Synonyms:benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside

Chemical Property of benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside

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Technology Process of benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside

There total 2 articles about benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

benzyl 2-acetamido-4-azido-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside (68536-11-8) → benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside (81997-64-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 760 Torr;

DOI:10.1016/S0008-6215(82)80016-5

Reference yield: 74.0%

benzyl 2-acetamido-4-azido-3-O-benzyl-2,4,6-trideoxy-α-D-glucopyranoside (50908-20-8) → benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-glucopyranoside (81997-64-0,138800-26-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 760 Torr;

DOI:10.1016/S0008-6215(82)80016-5

Reference yield: 55.0%

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + benzyl 2-acetamido-4-amino-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside (81997-64-0) → benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4-(2,4-dinitroanilino)-α-D-galactopyranoside (81997-60-6)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; for 3h; Ambient temperature;

DOI:10.1016/S0008-6215(82)80016-5

upstream raw materials:

benzyl 2-acetamido-4-azido-3-O-benzyl-2,4,6-trideoxy-α-D-glucopyranoside

benzyl 2-acetamido-4-azido-3-O-benzyl-2,4,6-trideoxy-α-D-galactopyranoside

Downstream raw materials:

benzyl 2-acetamido-3-O-benzyl-4-(2,4-dinitroanilino)-α-D-glucopyranoside

benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4-(2,4-dinitroanilino)-α-D-galactopyranoside

benzyl 2,4-diacetamido-3-O-benzyl-2,4,6-trideoxy-α-D-galactoside

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