Technology Process of C34H29(2)H5O6
There total 4 articles about C34H29(2)H5O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
at -35 ℃;
for 0.75h;
DOI:10.1039/b304411d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: KMnO4 / acetone / 1 h / 20 °C
2: diethyl ether / 0.05 h / 0 °C
3: LiAl(2)H4 / diethyl ether / 0.67 h / -35 °C
4: PBr3 / diethyl ether / 1 h / 20 °C
5: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C
With
potassium permanganate; lithium aluminium deuteride; phosphorus tribromide; lithium hexamethyldisilazane;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; acetone;
DOI:10.1039/b304411d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether / 0.05 h / 0 °C
2: LiAl(2)H4 / diethyl ether / 0.67 h / -35 °C
3: PBr3 / diethyl ether / 1 h / 20 °C
4: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C
With
lithium aluminium deuteride; phosphorus tribromide; lithium hexamethyldisilazane;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1039/b304411d