(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

Base Information

Chemical Name:(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid
CAS No.:73043-23-9
Molecular Formula:C₁₃H₁₂N₂O₄
Molecular Weight:260.249
Hs Code.:

Synonyms:(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

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Chemical Property of (Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

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Technology Process of (Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

There total 11 articles about (Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 935676-57-6
C₁₆H₁₆N₂O₅

: 73043-23-9
(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

Guidance literature:: With lithium hydroxide; In methanol; at 20 ℃; for 2h;
DOI:10.1002/ejoc.200600729

Reference yield: 44.0%

: (Z)-ethyl 2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetate

: 73043-23-9
(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

Guidance literature:: With hydrogenchloride; In acetic acid; for 7h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2016.10.016

Reference yield:

: 935676-55-4
C₁₆H₁₈N₂O₆

: 73043-23-9
(Z)-2-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihihydro-1H-imidazol-1-yl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / 0.2 h / 200 °C

2: 52 percent / aq. LiOH / methanol / 2 h / 20 °C

With lithium hydroxide; In methanol;
DOI:10.1002/ejoc.200600729