N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide

Base Information

• Chemical Name: N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide
• CAS No.: 96227-97-3
• Molecular Formula: C₂₂H₂₁N₅O₄S
• Molecular Weight: 451.506

Synonyms:N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide

Chemical Property of N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide

Chemical Property:

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Technology Process of N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide

There total 1 articles about N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.0^3,7>nonan-4,5-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

toluene-4-sulfonic acid hydrazide (1576-35-8) + C15H13N3O3 (96227-96-2) → N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.03,7>nonan-4,5-dicarboximide (96227-97-3)

Guidance literature:

In ethanol; for 5h; Heating;

DOI:10.1021/ja00298a044

Reference yield: 39.0%

N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.03,7>nonan-4,5-dicarboximide (96227-97-3) → N-phenyl-4,5-diazatricyclo<4.3.0.03,7>non-8-en-4,5-dicarboximide (96227-98-4)

Guidance literature:

With sodium hydride; In toluene; for 7h; Heating;

DOI:10.1021/ja00298a044

Reference yield:

N-phenyl-8-<(p-tolylsulfonyl)hydrazono>-4,5-diazatricyclo<4.3.0.03,7>nonan-4,5-dicarboximide (96227-97-3) → 4,5,6,7-tetrahydro-1H-indazole (2305-79-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 39 percent / NaH / toluene / 7 h / Heating

2: 1.) KOH; 2.) CuCl₂ / 1.) isopropanol, reflux, 14 h; 2.) 6M NH₃, 5 deg C, 20 min

3: 2.) H₂ / 2.) 20percent Pd-C / 1.) 350 deg C, 20 Torr; 2.) EtOAc, 2 h

With potassium hydroxide; hydrogen; sodium hydride; copper dichloride; palladium on activated charcoal; In toluene;

DOI:10.1021/ja00298a044

upstream raw materials:

toluene-4-sulfonic acid hydrazide

C₁₅H₁₃N₃O₃

Downstream raw materials:

N-phenyl-4,5-diazatricyclo<4.3.0.0^3,7>non-8-en-4,5-dicarboximide

4,5,6,7-tetrahydro-1H-indazole

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