{palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

Base Information

Chemical Name:{palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}
CAS No.:111026-20-1
Molecular Formula:C₅₅H₄₄Fe₂N₂O₇P₄PdPt
Molecular Weight:1382.05
Hs Code.:

Synonyms:{palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

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Chemical Property of {palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

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Technology Process of {palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

There total 1 articles about {palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 82307-36-6
{palladium-platinum(Cl)2(μ-dppm)}*CH2Cl2

: 25875-19-8
K{iron(carbonyl)3nitrosyl}

: 111026-20-1
{palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

Guidance literature:: In tetrahydrofuran; byproducts: KCl, CO; Addn. of a K(Fe(CO)3NO) soln. to an orange suspn. of (PdPtCl2(μ-dppm)2)*CH2Cl2 (cooling (-78°C), N2, stirring), soln. turns deep blue-green at ambient temp., stirring (2.5 h).; Concg. in vac., filtering to remove KCl, addn. of pentane and cooling (-20°C) gives dark green powder, filtering, recrystn. (toluene/pentane), elem. anal.;

Reference yield: 87.0%

: 111026-20-1
{palladium-platinum(iron)2(carbonyl)3(μ3-carbonyl)2(nitrosyl)2(μ-dppm)2}

: 25875-19-8
K{iron(carbonyl)3nitrosyl}

: 111026-22-3
{palladium-platinum-iron(iodo)(μ3-carbonyl)2(nitrosyl)(μ-dppm)2}

Guidance literature:: With KI; In acetone; Addn. of solid KI to stirred soln. of PdPtFe2(CO)5(NO)2(μ-dppm)2, dark green soln. turns immediately red, stirring (1 h).; Evapn. of solvent in vac., washing with H2O of red solid residue, extg. with Et2O, further extg. with CH2Cl2 gives red soln., addn. of n-hexane, cooling to -20°C, elem. anal.;