4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-

Base Information

Chemical Name:4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-
CAS No.:100098-80-4
Molecular Formula:C15H18 N2 O3 . Cl H
Molecular Weight:310.776
Hs Code.:

Synonyms:100098-80-4;4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-;LS-99913

Suppliers and Price of 4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-

Chemical Property:

Vapor Pressure:3.56E-05mmHg at 25°C
Boiling Point:364.3°Cat760mmHg
Flash Point:174.1°C
Density:g/cm³
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:310.1084202
Heavy Atom Count:21
Complexity:423

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC(N=C(O1)C=CC2=CC(=CC=C2)[N+](=O)[O-])(C)C.Cl
Isomeric SMILES:CC1CC(N=C(O1)/C=C/C2=CC(=CC=C2)[N+](=O)[O-])(C)C.Cl

Technology Process of 4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)-

There total 3 articles about 4H-1,3-Oxazine, 5,6-dihydro-2-(2-(3-nitrophenyl)ethenyl)-4,4,6-trimethyl-, monohydrochloride, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100098-66-6
(E)-3-nitro-N-(3-hydroxy-1,1-dimethylbutyl) cinnamamide

: 100098-80-4
4,4,6-Trimethyl-2-[(E)-2-(3-nitro-phenyl)-vinyl]-5,6-dihydro-4H-[1,3]oxazine; hydrochloride

Guidance literature:: With thionyl chloride; In toluene; Ambient temperature;

Reference yield:

: 555-68-0,1772-76-5
(E)-3-Nitrocinnamic acid

: 100098-80-4
4,4,6-Trimethyl-2-[(E)-2-(3-nitro-phenyl)-vinyl]-5,6-dihydro-4H-[1,3]oxazine; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / benzene / 0.5 h / 45 - 50 °C

2: CH₂Cl₂ / 3 h / 0 °C

3: 84 percent / SOCl₂ / toluene / Ambient temperature

With thionyl chloride; In dichloromethane; toluene; benzene;

Reference yield:

: 35418-05-4,141236-48-8
(E)-3-nitrocinnamic acid chloride

: 100098-80-4
4,4,6-Trimethyl-2-[(E)-2-(3-nitro-phenyl)-vinyl]-5,6-dihydro-4H-[1,3]oxazine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 3 h / 0 °C

2: 84 percent / SOCl₂ / toluene / Ambient temperature

With thionyl chloride; In dichloromethane; toluene;