2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid

Base Information

• Chemical Name: 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid
• CAS No.: 1254581-81-1
• Molecular Formula: C₃₂H₂₉NO₁₁S
• Molecular Weight: 635.648

Synonyms:2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid

Chemical Property of 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid

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Technology Process of 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid

There total 1 articles about 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C35H35NO11S (1254581-82-2) → 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid (1254581-81-1)

Guidance literature:

C₃₅H₃₅NO₁₁S; With potassium hydroxide; In methanol; water; for 4h; Reflux;

With hydrogenchloride; In methanol; water; at 20 ℃;

DOI:10.1039/c001780a

Reference yield: 75.0%

terbium(III) nitrate hexahydrate + 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid (1254581-81-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → Tb(3+)*CH3C6H4SO2NHC(CH2OC6H4COO)3(3-)*2(CH3)2NCHO*2H2O=[Tb(CH3C6H4SO2NHC(CH2OC6H4COO)3)((CH3)2NCHO)(H2O)2]*(CH3)2NCHO

Guidance literature:

With ammonia; In ethanol; water; soln. of nitrate in EtOH/H2O (1/1) was added to soln. of ligand in EtOH/H2O in presence of dil. ammonia; stirred at room temp. for 8 h; filtered; washed (EtOH/H2O); dried (vac.); elem. anal.;

DOI:10.1039/c001780a

Reference yield: 72.0%

europium(III) nitrate hexahydrate + 2,2'-(2-((2-carboxyphenoxy)methyl)-2-(4-methylphenylsulfonamido)propane-1,3-diyl)bis(oxy)dibenzoic acid (1254581-81-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → [Eu2(CH3C6H4SO2NHC(CH2OC6H4COO)3)2((CH3)2NCHO)4]*2(CH3)2NCHO

Guidance literature:

With ammonia; In ethanol; water; soln. of nitrate in EtOH/H2O (1/1) was added to soln. of ligand in EtOH/H2O in presence of dil. ammonia; stirred at room temp. for 8 h; filtered; washed (EtOH/H2O); dried (vac.); elem. anal.;

DOI:10.1039/c001780a

upstream raw materials:

C₃₅H₃₅NO₁₁S

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