(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

Base Information

Chemical Name:(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid
CAS No.:586372-50-1
Molecular Formula:C₂₃H₃₀N₂O₂
Molecular Weight:366.503
Hs Code.:

Synonyms:(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

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Chemical Property of (2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

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Technology Process of (2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

There total 4 articles about (2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 586372-48-7
4-(1H-imidazol-1-yl)-13-cis-methylretinoate

: 586372-50-1
(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

Guidance literature:: With potassium hydroxide; In methanol; for 2h; Heating;
DOI:10.1021/jm0401457

Reference yield:

: 16760-45-5
(2Z,4E,6E,8E)-methyl 3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-en-1-yl)nona-2,4,6,8-tetraenoate

: 586372-50-1
(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: MnO₂ / CH₂Cl₂ / 24 h / 20 °C

2: 1.5 g / NaBH₄ / methanol / 0.5 h / 20 °C

3: 89.5 percent / acetonitrile / 0.5 h / 20 °C

4: 73 percent / aq. KOH / methanol / 2 h / Heating

With manganese(IV) oxide; potassium hydroxide; sodium tetrahydroborate; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm0401457

Reference yield:

: 71748-57-7,163955-59-7
(2Z,4E,6E,8E)-methyl 3,7-dimethyl-9-(2,6,6-trimethyl-3-oxocyclohex-1-en-1-yl)nona-2,4,6,8-tetraenoate

: 586372-50-1
(2Z,4E,6E,8E)-9-(3-(1H-imidazol-1-yl)-2,6,6-trimethylcyclohex-1-en-1-yl)-3,7-dimethylnona-2,4,6,8-tetraenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.5 g / NaBH₄ / methanol / 0.5 h / 20 °C

2: 89.5 percent / acetonitrile / 0.5 h / 20 °C

3: 73 percent / aq. KOH / methanol / 2 h / Heating

With potassium hydroxide; sodium tetrahydroborate; In methanol; acetonitrile;
DOI:10.1021/jm0401457