[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

Base Information

Chemical Name:[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine
CAS No.:912581-14-7
Molecular Formula:C₂₅H₃₁NO₂
Molecular Weight:377.527
Hs Code.:

Synonyms:[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

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Chemical Property of [2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

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Technology Process of [2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

There total 6 articles about [2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2-(1-Benzyloxymethyl-cyclohexa-2,5-dienyl)-eth-(Z)-ylidene]-((R)-2-methoxy-1-phenyl-ethyl)-amine

: 912581-14-7
[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ol0618353

Reference yield:

: 912581-48-7
2-(1-(hydroxymethyl)cyclohexa-2,5-dienyl)acetonitrile

: 912581-14-7
[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NaH; tetrabutylammonium iodide / various solvent(s); tetrahydrofuran / 5 h / 0 - 20 °C

2: 326 mg / DIBAL-H / toluene; hexane / -70 - 0 °C

3: sodium sulfate / CH₂Cl₂ / 4 h

4: 262 mg / NaBH₄ / methanol / 2 h / 20 °C

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium sulfate; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene;
DOI:10.1021/ol0618353

Reference yield:

: 912581-12-5
(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-acetaldehyde

: 912581-14-7
[2-(1-benzyloxymethyl-cyclohexa-2,5-dienyl)-ethyl]-(2-methoxy-1-phenyl-ethyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / CH₂Cl₂ / 4 h

2: 262 mg / NaBH₄ / methanol / 2 h / 20 °C

With sodium tetrahydroborate; sodium sulfate; In methanol; dichloromethane;
DOI:10.1021/ol0618353