Technology Process of C52H80N2O17
There total 7 articles about C52H80N2O17 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
DOI:10.1021/jm034233n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / CH2Cl2 / 16 h / 20 °C
2: tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C
With
tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm034233n
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid monohydrate / benzene / 4 h / Heating
2: acetonitrile / 16 h / 20 °C
3: 1.25 g / imidazole / dimethylformamide / 16 h / 20 °C
4: triethylamine / CH2Cl2 / 16 h / 20 °C
5: tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C
With
1H-imidazole; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triethylamine; acetonitrile;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm034233n