C₂₇H₂₃BrO

Base Information

Chemical Name:C₂₇H₂₃BrO
CAS No.:1413301-66-2
Molecular Formula:C₂₇H₂₃BrO
Molecular Weight:443.383
Hs Code.:

Synonyms:C₂₇H₂₃BrO

Suppliers and Price of C₂₇H₂₃BrO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₇H₂₃BrO

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₂₃BrO

There total 1 articles about C₂₇H₂₃BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 52315-08-9
3-benzyl-benzaldehyde

: 126950-40-1
3,3'-dibromodiphenylmethane

: 1413301-66-2
C₂₇H₂₃BrO

Guidance literature:: 3,3'-dibromodiphenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

3-benzyl-benzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2dt31288c

Reference yield: 79.6%

: 1413301-66-2
C₂₇H₂₃BrO

: C₂₇H₂₃Br

Guidance literature:: With chloro-trimethyl-silane; sodium iodide; In hexane; acetonitrile; at 20 ℃; for 6h;
DOI:10.1039/c2dt31288c

Reference yield:

: 1413301-66-2
C₂₇H₂₃BrO

: 949909-76-6
C₃₃H₂₁NO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide; chloro-trimethyl-silane / hexane; acetonitrile / 6 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sodium dichromate dihydrate / acetic acid / 5 h / Reflux

With n-butyllithium; chloro-trimethyl-silane; sodium dichromate dihydrate; sodium iodide; In tetrahydrofuran; hexane; acetic acid; acetonitrile;
DOI:10.1039/c2dt31288c