C₆₃H₉₆O₂₅Si

Base Information

• Chemical Name: C₆₃H₉₆O₂₅Si
• CAS No.: 1360882-23-0
• Molecular Formula: C₆₃H₉₆O₂₅Si
• Molecular Weight: 1281.53
• Mol file: 1360882-23-0.mol

Synonyms:C₆₃H₉₆O₂₅Si

Chemical Property of C₆₃H₉₆O₂₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₆₃H₉₆O₂₅Si

There total 2 articles about C₆₃H₉₆O₂₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

di-tert-butyl dicarbonate (24424-99-5) + 6-O-tert-butyldiphenylsilyl-D-trehalose (1253891-15-4) → C63H96O25Si (1360882-23-0)

Guidance literature:

With dmap; triethylamine; In acetonitrile; at 20 ℃; for 48h;

DOI:10.1002/chem.201101827

Reference yield:

TREHALOSE (99-20-7) + tert-butylchlorodiphenylsilane (58479-61-1) → C63H96O25Si (1360882-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0.83 h / 0 °C / Inert atmosphere

2: dmap; triethylamine / acetonitrile / 48 h / 20 °C

With 1H-imidazole; dmap; triethylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/chem.201101827

upstream raw materials:

di-tert-butyl dicarbonate

6-O-tert-butyldiphenylsilyl-D-trehalose

TREHALOSE

tert-butylchlorodiphenylsilane