2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine

Base Information

• Chemical Name: 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine
• CAS No.: 135967-16-7
• Molecular Formula: C₂₂H₃₁NO₃S₂Si
• Molecular Weight: 449.711

Synonyms:2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine

Chemical Property of 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine

Chemical Property:

Purity/Quality:

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Technology Process of 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine

There total 3 articles about 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester (105398-69-4) → 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine (135967-16-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent Spectr_. / CH₂Cl₂ / 0 - 5 °C

2: m-chloroperbenzoic acid

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1016/S0040-4039(00)92693-5

Reference yield:

1-(phenylsulfonyl)-1-(trimethylsilyl)ethene (69627-08-3) → 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine (135967-16-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent Spectr_. / CH₂Cl₂ / 0 - 5 °C

2: m-chloroperbenzoic acid

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1016/S0040-4039(00)92693-5

Reference yield:

2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine (135967-10-1) → 2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine (135967-16-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

DOI:10.1016/S0040-4039(00)92693-5

upstream raw materials:

2-(1-Benzenesulfonyl-2-cyclohexyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine

Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

1-(phenylsulfonyl)-1-(trimethylsilyl)ethene

Downstream raw materials:

Cyclohexylacetic acid

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