o-Iodobenzoic acid sodium salt

Base Information

• Chemical Name: o-Iodobenzoic acid sodium salt
• CAS No.: 2532-17-4
• Molecular Formula: C7H5 I O2 . Na
• Molecular Weight: 270.002
• Mol file: 2532-17-4.mol

Synonyms:Benzoicacid, 2-iodo-, sodium salt (9CI); Benzoic acid, o-iodo-, sodium salt (8CI);Sodium 2-iodobenzoate; Sodium o-iodobenzoate

Chemical Property of o-Iodobenzoic acid sodium salt

Chemical Property:

• PSA: 40.13000
• LogP: 0.65470

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Safety Statements: Moderately toxic by ingestion, intravenous, and intramuscular routes. When heated to decompos"> − and Na2O." target="_blank">Moderately toxic by ingestion, intravenous, and intramuscular routes. When heated to decompos

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of o-Iodobenzoic acid sodium salt

There total 1 articles about o-Iodobenzoic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Iodobenzoic acid (88-67-5) + 4-nitrophenol sodium salt (824-78-2) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + sodium ortho-iodobenzoate (2532-17-4)

Guidance literature:

With 1-butyl-2,3-dimethylimidazolium bis-(trifluoromethanesulfonyl)amide; In methanol; at 24.84 ℃; Reagent/catalyst; Equilibrium constant;

DOI:10.1021/jo100914p

Reference yield: 84.0%

bis(cyclopentadienyl)titanium dichloride (1271-19-8) + sodium ortho-iodobenzoate (2532-17-4) → (C5H5)2Ti(IC6H4COO)2

Guidance literature:

In benzene; mixt. of complex and Na-salt of benzoic acid in dry benzene was stirredfor 3-8 h at 30°C; filtered, filtrate was evapd., recrystd. from boiling benzene; elem. anal.;

Reference yield: 70.6%

zirconocene dichloride (1291-32-3) + sodium ortho-iodobenzoate (2532-17-4) → bis(η5-cyclopentadienyl)zirconium(IV)(o-IC6H4COO)chloride

Guidance literature:

In benzene; byproducts: NaCl; under N2; anhydrous sodium salt of acid, complex and benzene stirred for 10h at 30°C, pptn. of NaCl; filtered, concd. (reduced pressure), addn. of petroleum ether, recrystd. (benzene/petroleum ether), dried (vac.); elem. anal.;

DOI:10.1016/S0277-5387(00)86796-0

upstream raw materials:

2-Iodobenzoic acid

4-nitrophenol sodium salt

Downstream raw materials:

<4-(2-Jod-benzoyloxy)-buttersaeure>-butylester

o-cyanobenzoic acid, sodium salt

2-oxo-2-phenylethyl 2-iodobenzoate

1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione

Refernces