C₁₄H₂₁N₃O₃

Base Information

Chemical Name:C₁₄H₂₁N₃O₃
CAS No.:1025807-23-1
Molecular Formula:C₁₄H₂₁N₃O₃
Molecular Weight:279.339
Hs Code.:

C<sub>14</sub>H<sub>21</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₁₄H₂₁N₃O₃

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Chemical Property of C₁₄H₂₁N₃O₃

Chemical Property:

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Technology Process of C₁₄H₂₁N₃O₃

There total 4 articles about C₁₄H₂₁N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026065-02-0
(1-Phenylaminomethyl-pentyl)-carbamic acid methyl ester

: 1025807-23-1
C₁₄H₂₁N₃O₃

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 1h;
DOI:10.1021/jm960372b

Reference yield:

: 5665-74-7,16397-19-6
2-amino-1-hexanol

: 1025807-23-1
C₁₄H₂₁N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetonitrile / 16 h / Ambient temperature

2: oxalyl chloride, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 20 °C

3: NaBH₃CN / methanol / 16 h / Ambient temperature; pH 5-6

4: concd HCl, NaNO₂ / H₂O / 1 h / 0 °C

With hydrogenchloride; oxalyl dichloride; sodium cyanoborohydride; potassium carbonate; dimethyl sulfoxide; triethylamine; sodium nitrite; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm960372b

Reference yield:

: (1-Hydroxymethyl-pentyl)-carbamic acid methyl ester

: 1025807-23-1
C₁₄H₂₁N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 20 °C

2: NaBH₃CN / methanol / 16 h / Ambient temperature; pH 5-6

3: concd HCl, NaNO₂ / H₂O / 1 h / 0 °C

With hydrogenchloride; oxalyl dichloride; sodium cyanoborohydride; dimethyl sulfoxide; triethylamine; sodium nitrite; In methanol; dichloromethane; water;
DOI:10.1021/jm960372b