apigenin-7-O-β-D-lactoside

Base Information

• Chemical Name: apigenin-7-O-β-D-lactoside
• CAS No.: 1389307-14-5
• Molecular Formula: C₂₇H₃₀O₁₅
• Molecular Weight: 594.526
• Mol file: 1389307-14-5.mol

Synonyms:apigenin-7-O-β-D-lactoside

Chemical Property of apigenin-7-O-β-D-lactoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of apigenin-7-O-β-D-lactoside

There total 6 articles about apigenin-7-O-β-D-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

apigenin-7-O-β-D-hepta-O-acetyllactoside (1389307-07-6) → apigenin-7-O-β-D-lactoside (1389307-14-5)

Guidance literature:

With water; ammonium hydroxide; In methanol; at 20 ℃; for 12h;

DOI:10.1016/j.carres.2012.05.013

Reference yield:

4'-O-benzylapigenin-7-O-β-D-hepta-O-acetyllactoside → apigenin-7-O-β-D-lactoside (1389307-14-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

2: water; ammonium hydroxide / methanol / 12 h / 20 °C

With 5%-palladium/activated carbon; water; hydrogen; ammonium hydroxide; In methanol; ethyl acetate;

DOI:10.1016/j.carres.2012.05.013

Reference yield:

4′-O-benzylapigenin (52309-82-7) → apigenin-7-O-β-D-lactoside (1389307-14-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; potassium carbonate / chloroform / 12 h / 45 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

3: water; ammonium hydroxide / methanol / 12 h / 20 °C

With 5%-palladium/activated carbon; tetrabutylammomium bromide; water; hydrogen; potassium carbonate; ammonium hydroxide; In methanol; chloroform; ethyl acetate;

DOI:10.1016/j.carres.2012.05.013

upstream raw materials:

apigenin-7-O-β-D-hepta-O-acetyllactoside

4′-O-benzylapigenin

naringin