Technology Process of C42H49N2O10
There total 4 articles about C42H49N2O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-(1-ylooxy-2,2,6,6-tetramethyl-4-piperidinyloxycarbonyl)-L-phenylalanine; (6aS,12S,12aR,5′R)-12-deoxo-12-hydroxyrotenone;
With
dmap;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
With
dicyclohexyl-carbodiimide;
In
dichloromethane;
for 4h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.024
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid
2.1: magnesium oxide / 24 h
3.1: dmap / dichloromethane / 0.08 h / 20 °C / Inert atmosphere
3.2: 4 h / Inert atmosphere
With
dmap; magnesium oxide; toluene-4-sulfonic acid;
In
dichloromethane;
DOI:10.1016/j.bmcl.2011.12.024
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate / methanol
2.1: dmap / dichloromethane / 0.08 h / 20 °C / Inert atmosphere
2.2: 4 h / Inert atmosphere
With
dmap; sodium tetrahydroborate;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.024