2,5,5,-trimethylhept-1,6-dien-4-ol

Base Information

Chemical Name:2,5,5,-trimethylhept-1,6-dien-4-ol
CAS No.:127808-17-7
Molecular Formula:C₁₀H₁₈O
Molecular Weight:154.252
Hs Code.:

Synonyms:2,5,5,-trimethylhept-1,6-dien-4-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5,5,-trimethylhept-1,6-dien-4-ol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2,5,5,-trimethylhept-1,6-dien-4-ol

There total 1 articles about 2,5,5,-trimethylhept-1,6-dien-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-63-3
prenyl bromide

: 27644-04-8,29887-38-5,57590-19-9,77363-66-7
(+-)-artemisia alcohol

: 127808-17-7
2,5,5,-trimethylhept-1,6-dien-4-ol

Guidance literature:: With acetic acid; zinc; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 2.) irradiation;
DOI:10.1016/S0040-4039(00)70649-6

Reference yield:

: 127808-17-7
2,5,5,-trimethylhept-1,6-dien-4-ol

: 26532-22-9,28117-21-7,30346-21-5,30820-22-5,51937-29-2,54088-78-7,68225-45-6,108645-56-3
grandisol

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / coprous trifluormethanesulphonate-benzene complex / diethyl ether / 65 h / Irradiation

2: 94 percent / pyridinium chlorochromate / Celite / CH₂Cl₂ / 4 h / Ambient temperature

3: 80 percent / hydroxylamine hydrochloride, potassium carbonate / ethanol / 3 h / Heating

4: 1.) phosphorous pentachloride, 2,6-lutidine, 2.) KOH / 1.) ether, 2.) ethylene glycol-triethylene glycol, dimethyl ether, 200 degC, 38 h

5: LiAlH₄ / diethyl ether / 5 h / Ambient temperature

With 2,6-dimethylpyridine; potassium hydroxide; lithium aluminium tetrahydride; copper(I) trifluoromethanesulfonate benzene; phosphorus pentachloride; hydroxylamine hydrochloride; potassium carbonate; pyridinium chlorochromate; Celite; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)96088-0

Reference yield:

: 127808-17-7
2,5,5,-trimethylhept-1,6-dien-4-ol

: 68225-44-5
2-[(1S,2R)-1-methyl-2-(prop-1-en-2-yl)cyclobutyl]acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / coprous trifluormethanesulphonate-benzene complex / diethyl ether / 65 h / Irradiation

2: 94 percent / pyridinium chlorochromate / Celite / CH₂Cl₂ / 4 h / Ambient temperature

3: 80 percent / hydroxylamine hydrochloride, potassium carbonate / ethanol / 3 h / Heating

4: 1.) phosphorous pentachloride, 2,6-lutidine, 2.) KOH / 1.) ether, 2.) ethylene glycol-triethylene glycol, dimethyl ether, 200 degC, 38 h

With 2,6-dimethylpyridine; potassium hydroxide; copper(I) trifluoromethanesulfonate benzene; phosphorus pentachloride; hydroxylamine hydrochloride; potassium carbonate; pyridinium chlorochromate; Celite; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)96088-0