(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

Base Information

Chemical Name:(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate
CAS No.:131244-26-3
Molecular Formula:C₂₀H₂₀Cl₃IN₂O₇
Molecular Weight:633.652
Hs Code.:

Synonyms:(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

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Chemical Property of (+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

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Technology Process of (+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

There total 6 articles about (+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22509-74-6
N-ethoxycarbonylphthalimide

: 131244-26-3
(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / Na₂CO₃ / acetone / 48 h / Ambient temperature

2: 1) NaH / 1) methylene dichloride, 0 deg C, 2) 0 deg C, 1 h

3: 95 percent / N-iodosuccinimide / CHCl₃ / 24 h / 4 °C

4: 1) 7percent HClO₄, 2) H₂O, sodium hydrogen carbonate / 1) methylene dichloride, methanol, room temperature, 1-2 h, 2) pH 8, 1 h

5: pyridine / 12 h

With pyridine; N-iodo-succinimide; perchloric acid; water; sodium hydride; sodium hydrogencarbonate; sodium carbonate; In chloroform; acetone;
DOI:10.1039/P19900002255

Reference yield:

: 102698-40-8,109906-47-0
(1S,4R,5R,6R)-4-Amino-5,6-dimethoxy-cyclohex-2-enol

: 131244-26-3
(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / Na₂CO₃ / acetone / 48 h / Ambient temperature

2: 1) NaH / 1) methylene dichloride, 0 deg C, 2) 0 deg C, 1 h

3: 95 percent / N-iodosuccinimide / CHCl₃ / 24 h / 4 °C

4: 1) 7percent HClO₄, 2) H₂O, sodium hydrogen carbonate / 1) methylene dichloride, methanol, room temperature, 1-2 h, 2) pH 8, 1 h

5: pyridine / 12 h

With pyridine; N-iodo-succinimide; perchloric acid; water; sodium hydride; sodium hydrogencarbonate; sodium carbonate; In chloroform; acetone;
DOI:10.1039/P19900002255

Reference yield:

: 131244-19-4
(+/-)-5c,6t-dimethoxy-4c-phthalimidocyclohex-2-en-1r-ol

: 131244-26-3
(+/-)-3t-iodo-5c,6t-dimethoxy-4c-phthalimido-2c-trichloracetamidocyclohexyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH / 1) methylene dichloride, 0 deg C, 2) 0 deg C, 1 h

2: 95 percent / N-iodosuccinimide / CHCl₃ / 24 h / 4 °C

3: 1) 7percent HClO₄, 2) H₂O, sodium hydrogen carbonate / 1) methylene dichloride, methanol, room temperature, 1-2 h, 2) pH 8, 1 h

4: pyridine / 12 h

With pyridine; N-iodo-succinimide; perchloric acid; water; sodium hydride; sodium hydrogencarbonate; In chloroform;
DOI:10.1039/P19900002255