ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

Base Information

Chemical Name:ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate
CAS No.:1173982-98-3
Molecular Formula:C₁₈H₂₀Cl₂N₄O₂S
Molecular Weight:427.354
Hs Code.:

Synonyms:ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

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Chemical Property of ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

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Technology Process of ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

There total 4 articles about ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1173982-97-2
ethyl N-(2,6-diaminophenyl)-β-alaninate

: 6590-96-1
2, 4-dichlorophenyl isothiocyanate

: 1173982-98-3
ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2018.01.020

Reference yield:

: 606-21-3
1-chloro-2,6-dinitrobenzene

: 1173982-98-3
ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 2 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 6 h / 20 °C

3: tetrahydrofuran / 1 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran;
DOI:10.1016/j.bmc.2018.01.020

Reference yield:

: 1173982-96-1
ethyl N-(2,6-dinitrophenyl)-β-alaninate

: 1173982-98-3
ethyl N-[2-amino-6-({[(2,4-dichlorophenyl)amino]carbonothioyl}amino)phenyl]-β-alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 6 h / 20 °C

2: tetrahydrofuran / 1 h / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran;
DOI:10.1016/j.bmc.2018.01.020