allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate

Base Information

• Chemical Name: allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate
• CAS No.: 1225450-81-6
• Molecular Formula: C₇₉H₉₂O₂₂S
• Molecular Weight: 1425.65

Synonyms:allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate

Chemical Property of allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate

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Technology Process of allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate

There total 1 articles about allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C117H120O22S (1225450-80-5) → allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate (1225450-81-6)

Guidance literature:

With formic acid; water; In methanol; dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.carres.2009.12.024

Reference yield:

allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate (1225450-81-6) → C79H88O22S

Guidance literature:

allyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-α-D-galactopyranosyl-(1->4)-[2,3-di-O-(4-methoxyphenylmethyl)-1-thio-α-Δ-^5,5a-carba-D-galactopyranosyl]-(1->4)-[methyl 2,3-di-O-(4-methoxyphenylmethyl)-α-D-galactopyranosid]urinate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.666667h;

With triethylamine; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1016/j.carres.2009.12.024

upstream raw materials:

C₁₁₇H₁₂₀O₂₂S

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