Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

Base Information

Chemical Name:Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide
CAS No.:199340-33-5
Molecular Formula:C₂₇H₄₉N₅O₃
Molecular Weight:491.718
Hs Code.:

Synonyms:Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

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Chemical Property of Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

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Technology Process of Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

There total 9 articles about Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 199340-32-4
(3-tert-Butoxycarbonylamino-propyl)-[4-(tert-butoxycarbonyl-{3-[(S)-2-heptanoylamino-3-(4-methoxy-phenyl)-propionylamino]-propyl}-amino)-butyl]-carbamic acid tert-butyl ester

: 199340-33-5
Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 12h;
DOI:10.1016/S0968-0896(97)00137-5

Reference yield:

: 71-44-3
Spermine

: 199340-33-5
Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / tetrahydrofuran / 5 h / Ambient temperature

2: Et₃N / methanol / Ambient temperature

3: 92 percent / H₂ / 10percent Pd/C / methanol / 4 h

4: 97 percent / K₂CO₃ / acetone / 8 h / Heating

5: 100 percent / TFA / CH₂Cl₂ / 12 h

With hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1016/S0968-0896(97)00137-5

Reference yield:

: 16652-64-5
O-benzyl-S-tyrosine

: 199340-33-5
Heptanoic acid [(S)-1-{3-[4-(3-amino-propylamino)-butylamino]-propylcarbamoyl}-2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / 1N aq. NaOH / tetrahydrofuran / 4 h / Ambient temperature

2: tetrahydrofuran / 0.5 h

3: Et₃N / tetrahydrofuran / 5 h / Ambient temperature

4: Et₃N / methanol / Ambient temperature

5: 92 percent / H₂ / 10percent Pd/C / methanol / 4 h

6: 97 percent / K₂CO₃ / acetone / 8 h / Heating

7: 100 percent / TFA / CH₂Cl₂ / 12 h

With sodium hydroxide; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1016/S0968-0896(97)00137-5