C₅₉H₆₃NO₃SSi₂

Base Information

Chemical Name:C₅₉H₆₃NO₃SSi₂
CAS No.:1618093-21-2
Molecular Formula:C₅₉H₆₃NO₃SSi₂
Molecular Weight:922.391
Hs Code.:

C<sub>59</sub>H<sub>63</sub>NO<sub>3</sub>SSi<sub>2</sub>

Synonyms:C₅₉H₆₃NO₃SSi₂

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Chemical Property of C₅₉H₆₃NO₃SSi₂

Chemical Property:

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Technology Process of C₅₉H₆₃NO₃SSi₂

There total 4 articles about C₅₉H₆₃NO₃SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1618093-17-6
C₅₄H₆₀BrNO₂Si₂

: 349616-56-4
5-(1,3-dioxolan-2-yl)-2-(tributylstannyl)thiophene

: 1618093-21-2
C₅₉H₆₃NO₃SSi₂

Guidance literature:: C₅₄H₆₀BrNO₂Si₂; 5-(1,3-dioxolan-2-yl)-2-(tributylstannyl)thiophene; With trans-bis(triphenylphosphine)palladium dichloride; N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;

With acetic acid; In tetrahydrofuran; water; at 60 ℃;
DOI:10.1016/j.dyepig.2014.04.043

Reference yield:

: 1618093-14-3
C₃₂H₄₄Br₂O₂Si₂

: 1618093-21-2
C₅₉H₆₃NO₃SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; toluene / 80 °C / Inert atmosphere

2.1: trans-bis(triphenylphosphine)palladium dichloride; N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2.2: 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; toluene; 1.1: |Suzuki-Miyaura Coupling / 2.1: |Stille Cross Coupling;
DOI:10.1016/j.dyepig.2014.04.043

Reference yield:

: 267220-47-3
4,8-dehydrobenzo[l,2-b:4,5-b′]difuran-4,8-dione

: 1618093-21-2
C₅₉H₆₃NO₃SSi₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; tin(ll) chloride; acetic acid / tetrahydrofuran / 60 °C / Inert atmosphere

2.1: n-butyllithium; carbon tetrabromide / tetrahydrofuran / -78 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; toluene / 80 °C / Inert atmosphere

4.1: trans-bis(triphenylphosphine)palladium dichloride; N,N-dimethyl-formamide / 90 °C / Inert atmosphere

4.2: 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; carbon tetrabromide; potassium carbonate; acetic acid; N,N-dimethyl-formamide; tin(ll) chloride; In tetrahydrofuran; toluene; 3.1: |Suzuki-Miyaura Coupling / 4.1: |Stille Cross Coupling;
DOI:10.1016/j.dyepig.2014.04.043