N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine

Base Information

• Chemical Name: N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine
• CAS No.: 959843-67-5
• Molecular Formula: C₂₇H₂₅N₅O₆
• Molecular Weight: 515.525

Synonyms:N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine

Chemical Property of N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine

Chemical Property:

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Technology Process of N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine

There total 1 articles about N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose (444019-07-2) + N-benzoyladenine (4005-49-6) → N6-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine (959843-67-5)

Guidance literature:

N-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide;

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; Further stages.;

DOI:10.1080/15257770701521730

Reference yield: 90.0%

N6-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine (959843-67-5) → 9-(5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine (1065271-32-0)

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; at 20 ℃; for 72h;

DOI:10.1016/j.bmc.2008.06.011

Reference yield:

N6-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine (959843-67-5) → 9-(5-O-benzoyl-2,3-dideoxy-3-C-methyl-β-D-erythro-pentofuranosyl)adenine (1058243-77-8)

Guidance literature:

N⁶-benzoyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine; With pyridine; acetic acid; hydrazine;

With dmap; phenylcarbonochloridothioate; In dichloromethane;

With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; Further stages.; Heating;

DOI:10.1080/15257770701521730

upstream raw materials:

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose

N-benzoyladenine

Downstream raw materials:

9-(5-O-benzoyl-2,3-dideoxy-3-C-methyl-β-D-erythro-pentofuranosyl)adenine

9-(5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)adenine

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