(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

Base Information

Chemical Name:(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol
CAS No.:782485-29-4
Molecular Formula:C₁₅H₁₈O₃S
Molecular Weight:278.372
Hs Code.:

Synonyms:(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

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Technology Process of (Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

There total 9 articles about (Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (7-benzenesulfonyl-nona-2,7,8-trienyloxy)-tert-butyl-diphenyl-silane

: 782485-29-4
(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃;
DOI:10.1021/jo0488614

Reference yield:

: 100571-18-4
6-(tert-butyldimethylsiloxy)hex-2-yn-1-ol

: 782485-29-4
(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaBH₄; aq. NaOH; H₂ / Ni(OAc)2*4H₂O; ethylenediamine / ethanol / 1 h / 20 °C

2.1: imidazole / dimethylformamide / 2 h / 20 °C

3.1: 227 mg / PPTS / methanol; tetrahydrofuran / 20 °C

4.1: 100 percent / PPh₃; imidazole; I₂ / CH₂Cl₂ / 0 - 20 °C

5.1: n-BuLi / tetrahydrofuran; hexane; various solvent(s) / 1 h / -78 °C

5.2: hexane; tetrahydrofuran; various solvent(s) / -78 - 20 °C

6.1: 306 mg / PPTS / methanol; tetrahydrofuran / 20 °C

7.1: Et₃N / tetrahydrofuran / -78 °C

8.1: H₂O₂; (NH₄)6Mo₇O₂₄*4H₂O / ethanol / 0 °C

9.1: aq. HCl / methanol / 20 °C

With 1H-imidazole; hydrogenchloride; ammonium heptamolybdate; sodium hydroxide; sodium tetrahydroborate; n-butyllithium; hydrogen; dihydrogen peroxide; iodine; pyridinium p-toluenesulfonate; triethylamine; triphenylphosphine; nickel diacetate; ethylenediamine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0488614

Reference yield:

: 121353-83-1
Z-6-[[(1,1-dimethyletyl)dimethylsilyl]oxy]-2-hexen-1-ol

: 782485-29-4
(Z)-7-(phenylsulfonyl)-2,7,8-nonatrien-1-ol

Guidance literature:: Multi-step reaction with 8 steps

1.1: imidazole / dimethylformamide / 2 h / 20 °C

2.1: 227 mg / PPTS / methanol; tetrahydrofuran / 20 °C

3.1: 100 percent / PPh₃; imidazole; I₂ / CH₂Cl₂ / 0 - 20 °C

4.1: n-BuLi / tetrahydrofuran; hexane; various solvent(s) / 1 h / -78 °C

4.2: hexane; tetrahydrofuran; various solvent(s) / -78 - 20 °C

5.1: 306 mg / PPTS / methanol; tetrahydrofuran / 20 °C

6.1: Et₃N / tetrahydrofuran / -78 °C

7.1: H₂O₂; (NH₄)6Mo₇O₂₄*4H₂O / ethanol / 0 °C

8.1: aq. HCl / methanol / 20 °C

With 1H-imidazole; hydrogenchloride; ammonium heptamolybdate; n-butyllithium; dihydrogen peroxide; iodine; pyridinium p-toluenesulfonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0488614