6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

Base Information

Chemical Name:6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol
CAS No.:118916-50-0
Molecular Formula:C₃₈H₄₆O₉
Molecular Weight:646.778
Hs Code.:

Synonyms:6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

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Chemical Property of 6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

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Technology Process of 6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

There total 1 articles about 6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 118798-71-3,118916-51-1,118916-52-2,118916-53-3
2,6-Anhydro-1,3,4-tri-O-benzyl-5-desoxy-8,9:10,11-di-O-isopropyliden-5-phenylsulfinyl-L-gulo-D-arabino-undec-5-enitol

: 118916-50-0
6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

Guidance literature:: With nickel; In tetrahydrofuran; for 1h; Ambient temperature;

Reference yield:

: 118916-50-0
6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

: 118916-54-4
2,6-Anhydro-1,3,4-tri-O-benzyl-8,9:10,11-di-O-isopropyliden-L-gulo-D-ido-D-glycero-undecitol

Guidance literature:: With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide; Yield given. Multistep reaction; 1.) THF, 10 h, 0 deg C, 2.) THF, 30 min, 0 deg C;

Reference yield:

: 118916-50-0
6,10-Anhydro-8,9,11-tri-O-benzyl-7-desoxy-1,2:3,4-di-O-isopropyliden-L-gulo-D-arabino-undec-5-enitol

: 118917-57-0
5,7-Di-O-acetyl-2,6-anhydro-1,3,4-tri-O-benzyl-8,9:10,11-di-O-isopropyliden-L-gulo-D-ido-D-glycero-undecitol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2 M Me₂S-BH₃, 2.) 10percent NaOH, 30percent H₂O₂ / 1.) THF, 10 h, 0 deg C, 2.) THF, 30 min, 0 deg C

2: 89 percent / pyridine / 8 h / Ambient temperature

With pyridine; sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide;