C₄₅H₈₀O₆Si₂

Base Information

Chemical Name:C₄₅H₈₀O₆Si₂
CAS No.:1261359-82-3
Molecular Formula:C₄₅H₈₀O₆Si₂
Molecular Weight:773.298
Hs Code.:

C<sub>45</sub>H<sub>80</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₅H₈₀O₆Si₂

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Chemical Property of C₄₅H₈₀O₆Si₂

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Technology Process of C₄₅H₈₀O₆Si₂

There total 41 articles about C₄₅H₈₀O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1261359-68-5
C₂₀H₃₈O₂Si

: 1261359-67-4
C₂₅H₄₂O₄Si

: 1261359-82-3
C₄₅H₈₀O₆Si₂

Guidance literature:: C₂₀H₃₈O₂Si; With n-butyllithium; In hexane; tert-butyl methyl ether; at -100 - 0 ℃; for 0.166667h; Inert atmosphere;

C₂₅H₄₂O₄Si; In hexane; tert-butyl methyl ether; at -100 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201204527

Reference yield:

: 1261359-68-5
C₂₀H₃₈O₂Si

: 1261359-67-4
C₂₅H₄₂O₄Si

: 1261359-82-3
C₄₅H₈₀O₆Si₂

: C₄₅H₈₀O₆Si₂

Guidance literature:: C₂₀H₃₈O₂Si; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -50 ℃; for 0.166667h;

C₂₅H₄₂O₄Si; In tetrahydrofuran; hexane; for 1.5h;
DOI:10.1021/ol1028699

Reference yield:

: 1261359-78-7
(2S,6S)-6-hexyl-2-(hydroxymethyl)tetrahydropyran

: 1261359-82-3
C₄₅H₈₀O₆Si₂

: C₄₅H₈₀O₆Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

1.2: 1.33 h / -78 - -20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 2 h

3.1: 4-Bromobenzoic acid; di-isopropyl azodicarboxylate; triphenylphosphine / diethyl ether / 16 h / 20 °C

3.2: 4 h / 20 °C

4.1: 1H-imidazole / dichloromethane / 16 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 - -50 °C

5.2: 1.5 h

With 1H-imidazole; n-butyllithium; oxalyl dichloride; 4-Bromobenzoic acid; di-isopropyl azodicarboxylate; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol1028699