C₃₁H₄₄N₄O₅Si

Base Information

Chemical Name:C₃₁H₄₄N₄O₅Si
CAS No.:1333433-82-1
Molecular Formula:C₃₁H₄₄N₄O₅Si
Molecular Weight:580.8
Hs Code.:

C<sub>31</sub>H<sub>44</sub>N<sub>4</sub>O<sub>5</sub>Si

Synonyms:C₃₁H₄₄N₄O₅Si

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Chemical Property of C₃₁H₄₄N₄O₅Si

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Technology Process of C₃₁H₄₄N₄O₅Si

There total 1 articles about C₃₁H₄₄N₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1307304-23-9
C₂₁H₂₃BrN₄O₃

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 97674-02-7
tributyl(1-ethoxyvinyl)stannane

: 1333433-82-1
C₃₁H₄₄N₄O₅Si

Guidance literature:: C₂₁H₂₃BrN₄O₃; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Inert atmosphere;

(2-trimethylethylsilylethoxy)methyl chloride; In N,N-dimethyl-formamide; for 18h;

tributyl(1-ethoxyvinyl)stannane; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 100 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1333433-82-1
C₃₁H₄₄N₄O₅Si

: 1333433-83-2
C₂₉H₃₉BrN₄O₅Si

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; water; at 0 ℃; for 1h;

Reference yield:

: 1333433-82-1
C₃₁H₄₄N₄O₅Si

: 1307304-30-8
C₂₃H₂₅N₇O

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / water; tetrahydrofuran / 1 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 18 h

3.1: ammonium acetate / xylenes / 3 h / 140 °C / Sealed pressure vessel

4.1: trifluoroacetic acid / dichloromethane / 20 h

4.2: UCT (CHQAX₁₅M₂₅) exchange resin

With N-Bromosuccinimide; ammonium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile; xylenes;