C₄₃H₅₀N₈O₈S₄

Base Information

Chemical Name:C₄₃H₅₀N₈O₈S₄
CAS No.:1399362-70-9
Molecular Formula:C₄₃H₅₀N₈O₈S₄
Molecular Weight:935.183
Hs Code.:

C<sub>43</sub>H<sub>50</sub>N<sub>8</sub>O<sub>8</sub>S<sub>4</sub>

Synonyms:C₄₃H₅₀N₈O₈S₄

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Chemical Property of C₄₃H₅₀N₈O₈S₄

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Technology Process of C₄₃H₅₀N₈O₈S₄

There total 20 articles about C₄₃H₅₀N₈O₈S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1391396-88-5
C₄₄H₅₂N₈O₈S₄

: 1399362-70-9
C₄₃H₅₀N₈O₈S₄

Guidance literature:: C₄₄H₅₂N₈O₈S₄; With lithium hydroxide; In methanol; dichloromethane; at 20 ℃; for 8h;

In methanol; dichloromethane; water; pH=1; Acidic conditions;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1391396-62-5
C₁₉H₂₈N₄O₃S₃

: 1399362-70-9
C₄₃H₅₀N₈O₈S₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

3.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux

4.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

4.2: 3 h / 0 °C / Inert atmosphere

4.3: 3 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

5.2: pH 1 / Acidic conditions

6.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

7.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

7.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; dichloromethane; water; benzene; 1.1: Hantzsch thiazole synthesis / 1.2: Hantzsch thiazole synthesis / 4.1: Hantzsch thiazole synthesis / 4.2: Hantzsch thiazole synthesis / 4.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1391396-63-6
C₂₄H₃₂N₄O₅S₃

: 1399362-70-9
C₄₃H₅₀N₈O₈S₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

2.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux

3.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

3.2: 3 h / 0 °C / Inert atmosphere

3.3: 3 h / 20 °C / Inert atmosphere

4.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

4.2: pH 1 / Acidic conditions

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

6.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; dichloromethane; water; benzene; 3.1: Hantzsch thiazole synthesis / 3.2: Hantzsch thiazole synthesis / 3.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105