Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:151072-62-7
Molecular Formula:C₆₃H₅₉ClO₂₀
Molecular Weight:1171.6
Hs Code.:

Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Synonyms:Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

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Chemical Property of Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 11 articles about Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 38992-99-3
methyl 2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

: 151072-59-2
O-(2-O-Benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl chloride

: 151072-62-7
Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; toluene; for 1h; Ambient temperature;
DOI:10.1016/0008-6215(93)80061-I

Reference yield:

: 151123-93-2
Ethyl 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-glucopyranoside

: 151072-62-7
Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / pyridine / CH₂Cl₂ / 0.33 h / 0 °C

2: 84 percent / Cl₂ / CCl₄; CHCl₃ / 0.08 h / 0 °C

3: 84 percent / Ag₂CO₃, AgClO₄, molecular sieves 4A / CH₂Cl₂ / 6 h / Ambient temperature

4: 92 percent / thiourea, 2,6-dimethylpyridine / methanol; CH₂Cl₂ / Heating

5: 84 percent / silver triflate, DTBMP, molecular sieves 4A / CH₂Cl₂; toluene / 1 h / Ambient temperature

With pyridine; 2,6-dimethylpyridine; 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; silver perchlorate; chlorine; thiourea; silver carbonate; In methanol; tetrachloromethane; dichloromethane; chloroform; toluene;
DOI:10.1016/0008-6215(93)80061-I

Reference yield:

: 151123-92-1
Ethyl 4,6-O-benzylidene-1-thio-α-D-glucopyranoside

: 151072-62-7
Methyl O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / NEt₃ / CH₂Cl₂ / 2 h / Ambient temperature

2: 93 percent / pyridine / CH₂Cl₂ / 0.33 h / 0 °C

3: 84 percent / Cl₂ / CCl₄; CHCl₃ / 0.08 h / 0 °C

4: 84 percent / Ag₂CO₃, AgClO₄, molecular sieves 4A / CH₂Cl₂ / 6 h / Ambient temperature

5: 92 percent / thiourea, 2,6-dimethylpyridine / methanol; CH₂Cl₂ / Heating

6: 84 percent / silver triflate, DTBMP, molecular sieves 4A / CH₂Cl₂; toluene / 1 h / Ambient temperature

With pyridine; 2,6-dimethylpyridine; 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; silver perchlorate; chlorine; triethylamine; thiourea; silver carbonate; In methanol; tetrachloromethane; dichloromethane; chloroform; toluene;
DOI:10.1016/0008-6215(93)80061-I