4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

Base Information

Chemical Name:4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate
CAS No.:139009-93-1
Molecular Formula:C₇H₈O₃S*C₁₉H₂₉N₃O₅
Molecular Weight:551.661
Hs Code.:

4-acetamidophenyl-N<sup>2</sup>-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

Synonyms:4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

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Chemical Property of 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

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Technology Process of 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

There total 2 articles about 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 104-15-4
toluene-4-sulfonic acid

: 139009-73-7
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

: 139009-93-1
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 25 ℃; for 1h; under 2068.6 Torr;
DOI:10.1016/S0040-4020(01)80998-4

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 139009-93-1
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1-ethyl-<3-(dimethylamino)propyl>carbodiimide*HCl, 4-dimethylaminopyridine / CH₂Cl₂; dimethylformamide / 1) 0-5 deg C, 1 h, 2) 25 deg C, 3 h

2: 87 percent / H₂ / 10percent Pd-C / acetic acid / 1 h / 25 °C / 2068.6 Torr

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80998-4