2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Base Information

Chemical Name:2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside
CAS No.:754201-83-7
Molecular Formula:C₃₂H₃₈N₂O₂₂
Molecular Weight:802.654
Hs Code.:

Synonyms:2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Suppliers and Price of 2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Chemical Property:

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Technology Process of 2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

There total 3 articles about 2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-α,β-maltoside

: 754201-83-7
2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.carres.2004.05.019

Reference yield:

: 18464-08-9,66073-13-0,71623-44-4,101981-29-7,109922-72-7,109922-73-8,132287-75-3,132287-76-4,132287-78-6,132303-63-0,134311-82-3,134333-39-4
2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-D-glucopyranose

: 754201-83-7
2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / DABCO / dimethylformamide / 20 °C

2: 71 percent / K₂CO₃ / dimethylformamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.05.019

Reference yield:

: 3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4,20880-60-8
1,2,3,6,2',3',4',6'-octa-O-acetylmaltose

: 754201-83-7
2,4-dinitrophenyl 2,2',3,3',4',6,6'-hepta-O-acetyl-O-acetyl-α-maltoside

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NH₂NH₂*acetate / dimethylformamide / 0.33 h / 50 °C

2: 63 percent / DABCO / dimethylformamide / 20 °C

3: 71 percent / K₂CO₃ / dimethylformamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; hydrazinium monoacetate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.05.019