(2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate

Base Information

• Chemical Name: (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate
• CAS No.: 1448620-53-8
• Molecular Formula: C₁₈H₂₅NO₂
• Molecular Weight: 292.362

Synonyms:(2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate

Chemical Property of (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate

Chemical Property:

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Technology Process of (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate

There total 2 articles about (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2E,6E)-3,7-dimethyl-8-oxoocta-2,6-dien-1-yl acetate (37905-02-5) → (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d5-phenylamino)octa-2,6-dien-1-yl acetate (1448620-53-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

2: sodium tris(acetoxy)borohydride / tetrahydrofuran

With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; 1: |Wittig Olefination;

DOI:10.1002/jlcr.3049

Reference yield:

C18H18(2)H5NO2 → (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d5-phenylamino)octa-2,6-dien-1-yl acetate (1448620-53-8)

Guidance literature:

With sodium tris(acetoxy)borohydride; In tetrahydrofuran;

DOI:10.1002/jlcr.3049

Reference yield: 81.0%

(2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d5-phenylamino)octa-2,6-dien-1-yl acetate (1448620-53-8) → (2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d5-phenylamino)octa-2,6-dien-1-ol (1448620-55-0)

Guidance literature:

With potassium carbonate; In methanol; water; at 20 ℃;

DOI:10.1002/jlcr.3049

upstream raw materials:

(2E,6E)-3,7-dimethyl-8-oxoocta-2,6-dien-1-yl acetate

Downstream raw materials:

(2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-ol

(R)-methyl 2-amino-3-(((2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl)thio)propanoate

(R)-2-amino-3-(((2E,6E)-3,7-dimethyl-8-(2,3,4,5,6-d₅-phenylamino)octa-2,6-dien-1-yl)thio)propanoic acid

C₁₆H₁₇⁽²⁾H₅BrN

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