ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

Base Information

Chemical Name:ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate
CAS No.:1308253-49-7
Molecular Formula:C₁₆H₁₅N₃O₄S
Molecular Weight:345.379
Hs Code.:

Synonyms:ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

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Chemical Property of ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

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Technology Process of ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

There total 3 articles about ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70-23-5
ethyl Bromopyruvate

: C₁₁H₁₁N₃O₂S

: 1308253-49-7
ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

Guidance literature:: ethyl Bromopyruvate; C₁₁H₁₁N₃O₂S; In ethanol; water; Reflux;

With sodium acetate; In ethanol; water; Reflux; Cooling;
DOI:10.1016/j.tet.2011.03.011

Reference yield:

: 2-(benzylthio)-6-hydroxy-5-nitroso-pyrimidin-4(3H)-one

: 1308253-49-7
ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dithionite / ethanol; water / 20 °C / Darkness

2.1: ethanol; water / Reflux

2.2: Reflux; Cooling

With sodium dithionite; In ethanol; water;
DOI:10.1016/j.tet.2011.03.011

Reference yield:

: 148020-95-5
C₁₁H₁₀N₂O₂S

: 1308253-49-7
ethyl 2-(benzylsulfanyl)-4-oxo-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: cis-nitrous acid

2.1: sodium dithionite / ethanol; water / 20 °C / Darkness

3.1: ethanol; water / Reflux

3.2: Reflux; Cooling

With sodium dithionite; cis-nitrous acid; In ethanol; water;
DOI:10.1016/j.tet.2011.03.011