Technology Process of C24H32O4
There total 6 articles about C24H32O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; N-butylamine; copper(l) chloride;
In
water;
at 0 - 20 ℃;
for 1h;
DOI:10.1055/s-0031-1290130
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; silver nitrate / acetone / 0.5 h / 0 - 20 °C
2: hydroxylamine hydrochloride; N-butylamine; copper(l) chloride / water / 1 h / 0 - 20 °C
With
N-Bromosuccinimide; hydroxylamine hydrochloride; silver nitrate; N-butylamine; copper(l) chloride;
In
water; acetone;
2: Cadiot-Chodkiewicz procedure;
DOI:10.1055/s-0031-1290130
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / 0 °C
2: potassium carbonate / methanol / 12 h / 20 °C
3: N-Bromosuccinimide; silver nitrate / acetone / 0.5 h / 0 - 20 °C
4: hydroxylamine hydrochloride; N-butylamine; copper(l) chloride / water / 1 h / 0 - 20 °C
With
N-Bromosuccinimide; hydroxylamine hydrochloride; sulfur trioxide pyridine complex; potassium carbonate; silver nitrate; dimethyl sulfoxide; N-butylamine; triethylamine; copper(l) chloride;
In
methanol; dichloromethane; water; acetone;
1: Parikh-Doering oxidation / 4: Cadiot-Chodkiewicz procedure;
DOI:10.1055/s-0031-1290130
