E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide

Base Information

• Chemical Name: E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide
• CAS No.: 1155337-75-9
• Molecular Formula: C₃₆H₅₄ClNO₃Si
• Molecular Weight: 612.368

Synonyms:E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide

Chemical Property of E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide

Chemical Property:

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Technology Process of E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide

There total 1 articles about E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H28ClNOSi + lyngbic acid (70607-97-5) → E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide (1155337-75-9)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo9003103

Reference yield: 93.0%

di-tert-butyl dicarbonate (24424-99-5) + E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-7-methoxytetradec-4-enamide (1155337-75-9) → E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-N'-(tert-butoxycarbonyl)-7-methoxytetradec-4-enamide (1155337-81-7)

Guidance literature:

With dmap; In tetrahydrofuran; for 16h; Reflux;

DOI:10.1021/jo9003103

upstream raw materials:

lyngbic acid

Downstream raw materials:

E,(7S)-N-[(2Z)-(chloromethylene)-4-(tert-butyldiphenylsilyloxy)butyl]-N'-(tert-butoxycarbonyl)-7-methoxytetradec-4-enamide

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