C₁₆H₁₉N₃

Base Information

Chemical Name:C₁₆H₁₉N₃
CAS No.:1093063-94-5
Molecular Formula:C₁₆H₁₉N₃
Molecular Weight:253.347
Hs Code.:

C<sub>16</sub>H<sub>19</sub>N<sub>3</sub>

Synonyms:C₁₆H₁₉N₃

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Chemical Property of C₁₆H₁₉N₃

Chemical Property:

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Technology Process of C₁₆H₁₉N₃

There total 5 articles about C₁₆H₁₉N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1093063-93-4
C₂₃H₂₅N₃

: 1093063-94-5
C₁₆H₁₉N₃

Guidance literature:: C₂₃H₂₅N₃; With Proton Sponge; 2-Chloroethyl chloroformate; In dichloromethane; at 20 ℃; for 4h;

With methanol; for 4h; Heating / reflux;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1093063-94-5
C₁₆H₁₉N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / 168 h / 100 °C

1.2: pH 7

2.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 100 °C

3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dimethyl sulfoxide / 2 h / 100 °C

4.1: Proton Sponge; 2-Chloroethyl chloroformate / dichloromethane / 4 h / 20 °C

4.2: 4 h / Heating / reflux

With aluminum (III) chloride; Proton Sponge; potassium acetate; potassium carbonate; 2-Chloroethyl chloroformate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; dimethyl sulfoxide; 2.1: Suzuki Coupling / 3.1: Suzuki Coupling;

Reference yield:

: 1093063-92-3
1-benzyl-4-(4-bromo-phenyl)-4-methyl-piperidine

: 1093063-94-5
C₁₆H₁₉N₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 100 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dimethyl sulfoxide / 2 h / 100 °C

3.1: Proton Sponge; 2-Chloroethyl chloroformate / dichloromethane / 4 h / 20 °C

3.2: 4 h / Heating / reflux

With Proton Sponge; potassium acetate; potassium carbonate; 2-Chloroethyl chloroformate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; dimethyl sulfoxide; 1.1: Suzuki Coupling / 2.1: Suzuki Coupling;