C₁₁H₇BrFNO

Base Information

Chemical Name:C₁₁H₇BrFNO
CAS No.:1422252-08-1
Molecular Formula:C₁₁H₇BrFNO
Molecular Weight:268.085
Hs Code.:

Synonyms:C₁₁H₇BrFNO

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Chemical Property of C₁₁H₇BrFNO

Chemical Property:

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Technology Process of C₁₁H₇BrFNO

There total 1 articles about C₁₁H₇BrFNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 372-48-5
2-fluoropyridine

: 121219-03-2
4-bromo-3-fluorophenol

: 1422252-08-1
C₁₁H₇BrFNO

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 120 ℃; for 30h; Inert atmosphere;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 5419-55-6
Triisopropyl borate

: 1422252-08-1
C₁₁H₇BrFNO

: C₁₅H₁₇BFNO₃

Guidance literature:: C₁₁H₇BrFNO; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.666667h; Inert atmosphere;

Triisopropyl borate; at -78 - 20 ℃; for 3.5h;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 1422252-08-1
C₁₁H₇BrFNO

: 1422252-10-5
C₂₉H₂₇FN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C / Inert atmosphere

1.2: 3.5 h / -78 - 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / Inert atmosphere; Reflux

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; n-butyllithium; trifuran-2-yl-phosphane; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; hexane; water; 2.1: |Suzuki Coupling;
DOI:10.1139/cjc-2012-0319