2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

Base Information

Chemical Name:2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester
CAS No.:223764-34-9
Molecular Formula:C₄₆H₇₉ClO₆
Molecular Weight:763.583
Hs Code.:

Synonyms:2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

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Chemical Property of 2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

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Technology Process of 2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

There total 6 articles about 2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 223764-33-8
3,4-bis(dodecyloxy)-5-(11-(methacryloyl)oxyundecyloxy)benzoic acid

: 223764-34-9
2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃;
DOI:10.1002/(SICI)1521-3765(19990301)5:3<1070::AID-CHEM1070>3.0.CO;2-9

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 223764-34-9
2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 83.4 percent / K₂CO₃ / dimethylformamide / 4 h / 60 °C

3: pyridine / CH₂Cl₂ / 3 h / 0 °C

4: pyridine, H₂O, HCl / 0.17 h / Heating

5: 96.3 percent / SOCl₂, DMF / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; water; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(19990301)5:3<1070::AID-CHEM1070>3.0.CO;2-9

Reference yield:

: 96642-97-6
methyl 7-hydroxy-2,2-dimethylbenzo[d][1,3]dioxole-5-carboxylate

: 223764-34-9
2-methyl-acrylic acid 11-(5-chlorocarbonyl-2,3-bis-dodecyloxy-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 83.4 percent / K₂CO₃ / dimethylformamide / 4 h / 60 °C

3: pyridine / CH₂Cl₂ / 3 h / 0 °C

4: pyridine, H₂O, HCl / 0.17 h / Heating

5: 96.3 percent / SOCl₂, DMF / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; water; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(19990301)5:3<1070::AID-CHEM1070>3.0.CO;2-9