tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

Base Information

Chemical Name:tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate
CAS No.:1335490-27-1
Molecular Formula:C₁₉H₂₇ClN₆O₄S
Molecular Weight:470.98
Hs Code.:

Synonyms:tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

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Chemical Property of tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

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Technology Process of tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

There total 4 articles about tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2831-66-5
2,4-dichloro-1,3,5-triazine

: 1335490-31-7
C₁₆H₂₇N₃O₄S

: 1335490-27-1
tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; isopropyl alcohol; at -20 ℃; for 0.5h;

Reference yield:

: 58032-84-1
(3-nitrophenyl)methanesulfonyl chloride

: 1335490-27-1
tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 5.5 h / 20 °C

2: hydrogen / Raney-Ni / methanol / 36 h / 50 °C / 3750.38 Torr / Parr reactor

3: N-ethyl-N,N-diisopropylamine / isopropyl alcohol; tetrahydrofuran / 0.5 h / -20 °C

With pyridine; hydrogen; N-ethyl-N,N-diisopropylamine; Raney-Ni; In tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol;

Reference yield:

: 1335490-29-3
C₁₆H₂₅N₃O₆S

: 1335490-27-1
tert-butyl [4-(((3-((4-chloro-1,3,5-triazin-2-yl)amino)phenyl)methyl)sulfonamido)butyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / Raney-Ni / methanol / 36 h / 50 °C / 3750.38 Torr / Parr reactor

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol; tetrahydrofuran / 0.5 h / -20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; Raney-Ni; In tetrahydrofuran; methanol; isopropyl alcohol;