Technology Process of 2-(trimethylsilyl)ethoxymethyl phenyl selenide
There total 9 articles about 2-(trimethylsilyl)ethoxymethyl phenyl selenide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
diphenyl diselenide;
With
sodium tetrahydroborate;
In
N,N-dimethyl-formamide;
at 60 - 110 ℃;
Inert atmosphere;
(2-trimethylethylsilylethoxy)methyl chloride;
In
N,N-dimethyl-formamide;
at 35 ℃;
for 5h;
DOI:10.1016/j.tetlet.2011.04.036
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-iodo-succinimide; potassium carbonate / ethyl acetate / 20 °C / Inert atmosphere; Molecular sieve
2.1: sodium tetrahydroborate / N,N-dimethyl-formamide / 60 - 110 °C / Inert atmosphere
2.2: 5 h / 35 °C
With
sodium tetrahydroborate; N-iodo-succinimide; potassium carbonate;
In
ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.04.036
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-iodo-succinimide; potassium carbonate / ethyl acetate / 20 °C / Inert atmosphere; Molecular sieve
2.1: sodium tetrahydroborate / N,N-dimethyl-formamide / 60 - 110 °C / Inert atmosphere
2.2: 5 h / 35 °C
With
sodium tetrahydroborate; N-iodo-succinimide; potassium carbonate;
In
ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.04.036
