1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

Base Information

Chemical Name:1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene
CAS No.:162708-85-2
Molecular Formula:C₂₁H₂₉NO₄S
Molecular Weight:391.532
Hs Code.:

Synonyms:1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

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Chemical Property of 1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

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Technology Process of 1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

There total 5 articles about 1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 166672-55-5
(+/-)-1-(dimethylcarbamoyloxy)-3-phenylsulfonylmethyl-2,2,4-trimethyl-1-vinyl-3-cyclohexene

: 162708-85-2
1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

Guidance literature:: With mercury(II) trifluoroacetate; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(97)00411-0

Reference yield:

: 162708-84-1
(+/-)-1-(dimethylcarbamoyloxy)-2,2,4-trimethyl-3-phenylthiomethyl-1-vinyl-3-cyclohexene

: 162708-85-2
1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / MMPP / tetrahydrofuran / 2 h / Ambient temperature

2: 96 percent / Hg(OCOCF₃)2 / tetrahydrofuran / 3 h / Ambient temperature

With mercury(II) trifluoroacetate; In tetrahydrofuran;
DOI:10.1016/S0040-4020(97)00411-0

Reference yield:

: 162708-91-0
(+/-)-2,2,4-trimethyl-3-phenylthiomethyl-1-vinyl-3-cyclohexen-1-ol

: 162708-85-2
1E-<2-(dimethylcarbamoyloxy)ethylidene>-3-phenylsulfonylmethyl-2,2,4-trimethylcyclohex-3-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH / 1.) THF, room temperature, 16 h, 2.) 0 deg C, 3 h

2: 82 percent / MMPP / tetrahydrofuran / 2 h / Ambient temperature

3: 96 percent / Hg(OCOCF₃)2 / tetrahydrofuran / 3 h / Ambient temperature

With mercury(II) trifluoroacetate; potassium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(97)00411-0