sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

Base Information

Chemical Name:sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate
CAS No.:1381785-18-7
Molecular Formula:C₂₃H₁₇F₃N₃O₅S*Na
Molecular Weight:527.456
Hs Code.:

Synonyms:sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

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Chemical Property of sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

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Technology Process of sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

There total 6 articles about sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1381785-36-9
methyl 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

: 1381785-18-7
sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: With sodium hydroxide; In methanol; at 60 ℃; for 18h;

Reference yield:

: 1227268-77-0
3-methylimidazo[1,2-a]pyridine-2-carboxylic acid

: 1381785-18-7
sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; diphenylphosphoranyl azide / 1,2-dichloro-ethane / 18 h / 20 °C

1.2: 82 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

2.2: 2 h / 20 °C

3.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 18 h / 20 °C

5.1: sodium hydroxide / methanol / 18 h / 60 °C

With hydrogenchloride; diphenylphosphoranyl azide; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1381785-33-6
tert-Butyl (3-methylimidazo[1,2-a]pyridin-2-yl)carbamate

: 1381785-18-7
sodium 4-(N-(3-methylimidazo[1,2-a]pyridin-2-yl)-N-((4-trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 2 h / 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 18 h / 20 °C

4.1: sodium hydroxide / methanol / 18 h / 60 °C

With hydrogenchloride; sodium hydride; potassium carbonate; sodium hydroxide; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;