C₃₃H₅₂N₂O₈S

Base Information

Chemical Name:C₃₃H₅₂N₂O₈S
CAS No.:1280727-39-0
Molecular Formula:C₃₃H₅₂N₂O₈S
Molecular Weight:636.85
Hs Code.:

C<sub>33</sub>H<sub>52</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₃₃H₅₂N₂O₈S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₅₂N₂O₈S

Chemical Property:

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Technology Process of C₃₃H₅₂N₂O₈S

There total 6 articles about C₃₃H₅₂N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70-49-5,644-87-1
DL-thiomalic acid

: 1280727-38-9
C₂₉H₄₇ClN₂O₄

: 1280727-39-0
C₃₃H₅₂N₂O₈S

Guidance literature:: DL-thiomalic acid; C₂₉H₄₇ClN₂O₄; In ISOPROPYLAMIDE; at 20 ℃;

1,8-diazabicyclo[5.4.0]undec-7-ene; In ISOPROPYLAMIDE; at 30 - 60 ℃; for 5.5h;

With sodium hydroxide; In ISOPROPYLAMIDE; water; for 0.166667h; Product distribution / selectivity;

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1280727-39-0
C₃₃H₅₂N₂O₈S

Guidance literature:: Multi-step reaction with 6 steps

1.1: bromine; hydrogen bromide / water; methanol / 3.5 h / 30 - 34 °C

2.1: water; ISOPROPYLAMIDE / 4 h / 20 °C

3.1: methanol / Inert atmosphere

3.2: 8 h / 20 °C / Reflux

4.1: ISOPROPYLAMIDE / 5 h / 20 °C / Cooling with ice

5.1: trichlorophosphate / acetonitrile / 1 h / 0 - 5 °C

5.2: 4 h / 20 - 40 °C

6.1: ISOPROPYLAMIDE / 20 °C

6.2: 5.5 h / 30 - 60 °C

6.3: 0.17 h

With hydrogen bromide; bromine; trichlorophosphate; In methanol; ISOPROPYLAMIDE; water; acetonitrile;

Reference yield:

: 17687-64-8
2-(3-methyl-2-oxobutyl)isoindoline-1,3-dione

: 1280727-39-0
C₃₃H₅₂N₂O₈S

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / Inert atmosphere

1.2: 8 h / 20 °C / Reflux

2.1: ISOPROPYLAMIDE / 5 h / 20 °C / Cooling with ice

3.1: trichlorophosphate / acetonitrile / 1 h / 0 - 5 °C

3.2: 4 h / 20 - 40 °C

4.1: ISOPROPYLAMIDE / 20 °C

4.2: 5.5 h / 30 - 60 °C

4.3: 0.17 h

With trichlorophosphate; In methanol; ISOPROPYLAMIDE; acetonitrile;